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排序方式: 共有239条查询结果,搜索用时 15 毫秒
61.
62.
用PMS 30B型汞采样器采集固定污染源废气,再用塞曼原子吸收汞分析仪测定样品中的汞,高、低浓度汞标准样品测定结果均在标准范围内,相对误差分别为0和4.3%。汞吸收管对高、低浓度含汞废气的穿透效率表明,当废气汞质量浓度达到mg/m3级别时,穿透率仅为1.3%。用该方法测定稳定工况固定污染源废气中的汞,6次测定结果的RSD为5.9%,方法检出限为1.04 ng,当采样体积为20 L时,检出限为0.05μg/m3。实际监测表明,钢铁企业、燃煤电厂、垃圾焚烧厂废气中汞为0.07μg/m3~1 031μg/m3。 相似文献
63.
《Environmental Forensics》2013,14(1):27-34
Comprehensive two-dimensional gas chromatography, GC 2 GC, is a new analytical tool with a tremendous capability to separate and identify organic compounds in complex environmental samples. GC 2 GC uses two different chromatography columns coupled serially by a modulator to produce a volatility by polarity separation and distribute compound peaks across a two-dimensional retention time plane. The two-dimensional separation produces an order of magnitude more resolved peaks than traditional GC methods. The grouping or ordering of the peaks in the GC 2 GC chromatogram facilitates the identification of unknown compounds and the comparison of complex environmental samples. When a mass spectrometer detector is used, each resolved GC 2 GC peak yields a single-component, interference-free mass spectrum that leads to accurate matching with mass spectral libraries. GC 2 GC examination of marine sediment extracts identified a wide variety of chemical contaminants including polychlorinated biphenyls, p -nonylphenol isomers, polycyclic aromatic hydrocarbons, benzotriazoles, and the alkane, cycloalkane, alkylbenzene, alkylnaphthalene, and biomarker fractions of petroleum. The two-dimensional GC 2 GC chromatogram image permits rapid screening of the sediment extracts for these and other unknown contaminants. 相似文献
64.
n-Hexane is widely used in industrial production as an organic solvent. As an industrial exhaust gas, the contribution of n-hexane to air pollution and damage to human health are attracting increasing attention. In the present study, aqueous solutions of two fluorocarbon surfactants(FSN100 and FSO100) were investigated for their properties of solubilization and dynamic absorption of n-hexane, as well as their capacity for regeneration and n-hexane recovery by thermal distillation. The results show that the two fluorocarbon surfactants enhance dissolution and absorption of n-hexane, and their effectiveness is closely related to their concentrations in solution. For low concentration solutions(0.01%–0.30%), the partition coefficient decreases dramatically and the saturation capacity increases significantly with increasing concentration, but the changes for both are more modest when the concentration is over 0.30%. The FSO100 solution presents a smaller partition coefficient and a greater saturation capacity than the FSN100 solution at the same concentration,indicating a stronger solubilization for n-hexane. Thermal distillation is a feasible method to recover n-hexane from these absorption solutions, and to regenerate them. With 90 sec heating at 80–85°C, the recovery of n-hexane ranges between 81% and 85%, and the regenerated absorption solution maintains its original performance during reuse. This study provides basic information on two fluorocarbon surfactants for application in the treatment of industrial n-hexane waste gases. 相似文献
65.
基于在pH值为4.0~5.2的BR缓冲介质中,镉与刚果红发生显色反应并生成蓝色离子缔合物的原理,建立了测定垃圾渗滤液中镉的巯基棉分离富集光度法。其最大正吸收波长和最大负吸收波长分别为604nm和492nm,线性范围分别为0.10mg/L~2.80mg/L和0.10mg/L~3.40mg/L,采用双波长叠加测定灵敏度更高。探讨了渗滤液的处理方法及共存离子对测定的影响,优化了试验条件,实际样品的测定结果与原子吸收法对比无显著差异,加标回收率为98,6%~104%。 相似文献
66.
Mohammad Khan Jamali Tasneem Gul Kazi Mohammad Bilal Arain Hassan Imran Afridi Nusrat Jalbani Jameel A. Baig Abdul Niaz 《The Environmentalist》2008,28(4):366-375
The recycling of sewage sludge on agriculture land represents an alternative, advantageous, disposal of this waste material.
The aim of the present study was to evaluate the feasibility of using industrial sewage sludge, produced in Pakistan, as a
fertiliser. Agricultural soil amended with 25% (w/w) sewage sludge with or without lime treatment was used for growing a variety
of sorghum (PARC-SS-1). The mobility of the heavy metals (HMs) (Cd, Cu, Cr, Ni, Pb and Zn) and metalloid (As) in the untreated
industrial waste water sewage sludge (UIWS) samples were assessed by applying a modified BCR (Community Bureau of Reference)
sequential extraction procedure. The single extraction procedure comprised of the application of mild extractant (CaCl2) and water for the estimation of the proportion of easily soluble metal fractions. The precision and accuracy of BCR was
evaluated by using a certified reference material of soil amended with sewage sludge BCR 483. The plant available metal contents,
as extracted by the deionised water and 0.01 M CaCl2 solution and exchangeable fraction of BCR sequential, decreased with lime application in the range of 10–44% for As, Cr,
Ni, Pb and Zn, except in the cases of Cd and Cu, where their mobility was increased by 10% and 24%, respectively. Sludge amendment
enhanced the dry weight yield of sorghum and the increase was more obvious after liming up to 25%. The uptake of HMs were
lower in test samples (3.2–21.8%), except for Cu and Cd, which was higher (4%), while they were below the permissible limit
of these metals. The present experiment demonstrates that liming was important in factors facilitating the growth of sorghum
in sludge-amended soil. 相似文献
67.
武子 《环境监测管理与技术》1997,9(1):39-41
阐述了运用办公自动化应用软件电子表格Excel制作及播放新型声像片的方法,并以环境监测工作中的实例介绍了具体的制作过程。 相似文献
68.
用0.1%硝酸溶液配制混合标准溶液,不加抗干扰试剂,火焰原子吸收光谱法直接测定酸雨中K、Na、Ca、Mg,方法精密度、准确度满足酸雨监测的分析要求。 相似文献
69.
本文对分布面广而复杂的瓦斯泵房噪声源进行了测试和深入的分析,采用综合治理的方法使居民区噪声达到了国家城市环境噪声标准的要求,瓦斯泵房内降噪显著,取得了理想的治理效果。 相似文献
70.